Determination of trace hafnium in zirconium and zirconium alloys by inductively coupled plasma emission spectrometry
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Selective Separation and Preconcentration of trace Amounts of Gallium in Water and Rice Samples using Cloud Point Extraction and Determination by Inductively Coupled Plasma-Atomic Emission Spectrometry
In the present study a cloud-point extraction process using non-ionic surfactant Triton X-114 for selective extraction of gallium from aqueous solutions was developed. The method is based on the complex formation of Ga (III) with N, N′ -bis (salycilidene)-1, 2-phenylenediamine (salophen) as a chelating agent in buffer media of pH 5. After phase separation and dilution of the surfactant-rich pha...
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This rapid, accurate procedure for trace elements and electrolytes in serum requires little sample preparation: to 1 mL of serum a single reagent is added that contains trichloroacetic and hydrochloric acids for protein precipitation, hydroxylamine sulfate for iron reduction, and yttrium as the internal standard. After centrifugation, the supernates are directly analyzed for Na, K, Mg, Ca, Pi, ...
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A method for the determination of Ti and V using inductively coupled plasma atomic emission spectrometry (ICP OES) in Ziegler-Natta polymerization catalysts is proposed. The concentrations of both Ti and V are efficiently determined after catalyst acid digestion with a mixture of HNO3 + HCl + HF and heating (160 degrees C for 6 h) or with 10% (v/v) H2SO4 and heating (160 degrees C for 6 h) or w...
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ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 1982
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.31.8_413